International Science Community Association Research Journal of Chemical Sciences 15 4 2025 10 18 Synthesis, studying the spectral, thermal aspects and in vitro Antimicrobial activity of Novel Azo Co-ordination Polymers 7 14 EN Nainvi Brajesh 1 Department of Chemistry, V.S.S.D. College, Kanpur 208002 UP, India Singh Ashok 2 Department of Chemistry, V.S.S.D. College, Kanpur 208002 UP, India Lal Nand 3 Department of Chemistry, V.S.S.D. College, Kanpur 208002 UP, India Thakor Subhash B. 1 Shri PHG Muni, Arts & Science College, Gujarat University, Kalol–382721, Gujarat, India Patel V.G. 2 Department of Chemistry, Municipal Arts & Urban Bank Science College, Mehsana, Gujarat, India > Research Paper 2025 5 18 2025 10 18 4,6-Dinitroresorcinol was reduced in alcoholic alkali to give a novel azo polymer, poly [azo(1-napthol)]. These co-ordinationpolymers of polyazochelates we reprepared with cu+2, Ni+2, Co+2, Mn+2 and Zn+2 metal ions. The novel polymer synthesized at Batch: 1 were characterized by following techniques such as elemental analysis, IR spectra & thermo gravimetric analysis. The co-ordination polymers were characterized by elemental Analysis, IR spectral and diffuse reflectance spectral studies and were evaluated for their thermalst ability by thermogravimetric Analysis. The number average molecular weight (Mn) was determined by non aqueous conductometric titration. Furthermore, the magnetic susceptibilities of these coordination polymers have been examined. Antimicrobial efficacy of all these compound also been scrutinized. Copyright@ International Science Community Association